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Structural properties of amorphous and nanocrystallized Fe-Cu-Nb-Si-B and Fe-Gd-Cu-Nb-Si-B ribbons

Domenii publicaţii > Fizica + Tipuri publicaţii > Articol în revistã ştiinţificã

Autori: Ovidiu Crisan, Le Breton JM, Jianu A, Teillet J, Filoti G

Editorial: JOURNAL OF ALLOYS AND COMPOUNDS, 262, p.381-389, 1997.


The influence of Gd addition on the structural properties of Fe-Cu-Nb-Si-B nanocrystallized and amorphous alloys is studied. The crystallization temperature increases and the microstructure of the annealed samples changes. Gd addition induces the formation of Gd-Fe-B phases. In fully crystallized Fe-Gd-Cu-Nb-Si-B alloys the alpha-Fe(Si), Fe-Nb-B, Gd3Fe62B14 and Gd1.1Fe4B4 phases are observed. The evolution of the microstructure is followed as a function of the cumulative effects of annealing time and temperature. The results suggest the transformation of the metastable Gd3Fe62B14 phase into Gd1.1Fe4B4 and alpha-Fe. The hyperfine parameters of the Gd3Fe62B14 Mossbauer contribution are reported.

Cuvinte cheie: Fe-Cu-Nb-Si-B ribbons; Gd addition; melt spinning; nanostructure; Mossbauer spectrometry