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Sinteza de glicozilsulfone in conditiile CTI

Domenii publicaţii > Chimie + Tipuri publicaţii > Articol în revistã ştiinţificã

Autori: I.Sisu,N.Dinca,E.Sisu

Editorial: Rev.Chim., 57(6), p.615-618, 2006.

Rezumat:

The synthesis of glycosyl sulphone in PTC conditions using dioxirane generated in situ are presented. The yields of the oxidations in PTC conditions (60-81%) are comparable with those of reactions using NaIO4 and RuCl3 as catalyst. The synthesised glycosyl sulphone have been characterized by Chemical Ionization – Mass Spectrometry (CI-MS), 1H-NMR spectroscopy and melting point.

Cuvinte cheie: Phase transfer catalisys, S-glycosyl sulphone, Oxone@, dioxiran,